Ethyl 3-phenylprop-2-enoate → Ethyl 3-phenylpropionate

HRID 1388581Notes

Reaction equation

HRID 1388581 reaction equation
[C:1]([O:11][CH2:12][CH3:13])(=[O:10])[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[H][H]>C(O)C>[C:4]1([CH2:3][CH2:2][C:1]([O:11][CH2:12][CH3:13])=[O:10])[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

Participants

4

Reactant 2

HCID 7649Ethyl 3-phenylprop-2-enoateHCID 178418361HCID 178418361, compound

Product 1

HCID 16237Ethyl 3-phenylpropionate

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 30 g ethyl cinnamate in 100 ml ethanol containing 2.0 g catalyst, as prepared in Example 3, in a 250 ml stainless steel autoclave may be hydrogenated at 1200 psig hydrogen and 170° C. for about 1.5 hr. to afford ethyl 3-phenylpropionate.

Sources & evidence

ORD record
ord-821b8062f4ed4ca4a89a46c5e91e9f40
Source dataset
uspto-grants-1984_02
Patent number
US04431836

Reaction notes

Loading…