HCID 20471370, compound → HCID 13067095, compound

HRID 1388600Notes

Reaction equation

HRID 1388600 reaction equation
[Cl:1][C:2]1[CH:23]=[CH:22][C:5]2[C:6]3[CH:20]([CH3:21])[N:19]=[CH:18][C:7]=3[CH2:8][N:9]=[C:10]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=3[F:17])[C:4]=2[CH:3]=1.ClC1C=CC2C3C(=CNC=3)CN=C(C3C=CC=CC=3F)C=2C=1>>[Cl:1][C:2]1[CH:23]=[CH:22][C:5]2[C:6]3[C:7](=[CH:18][NH:19][C:20]=3[CH3:21])[CH2:8][N:9]=[C:10]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=3[F:17])[C:4]=2[CH:3]=1

Participants

3

Reactant 2

HCID 20471370HCID 20471370, compoundHCID 136045442HCID 136045442, compound

Product 1

HCID 13067095HCID 13067095, compound

Procedure

The preparation of 8-chloro-6-(2-fluorophenyl)-1-methyl-1H,4H-pyrrolo[3,4-d][2]benzazepine was conducted in the same manner as the preparation of 8-chloro-6-(2-fluorophenyl)-2H,4H-pyrrolo[3,4-d][2]benzazepine to give colorless prisms, mp 226°-227°.

Workup

  1. customto give colorless prisms, mp 226°-227°

Sources & evidence

ORD record
ord-40382330d9564aa2a27d89d8f5c29d54
Source dataset
uspto-grants-1984_02
Patent number
US04431823

Reaction notes

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