HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13279117, compound → 2-chloromethyl 7-amino 2,3-dihydro [4H] 1,4-benzodioxin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13279117 | HCID 13279117 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-chloromethyl 7-amino 2,3-dihydro [4H] 1,4-benzodioxin | HCID 13279118 | — |
Reaction Steps
150 g of 2-chloromethyl 7-nitro 2,3-dihydro [4H] 1,4-benzodioxin are dissolved in 2600 ml ethanol. 15 g of palladium on coal are added and the whole mixture is hydrogenated at room temperature and atmospheric pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04432984 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-d3e324b96a6943bf8165a609146d38c6 |
| Source note | uspto-grants-1984_02 |