HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 5-Chloromethylfurfural
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | D-(-)-Fructose | HCID 5984 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 5-Chloromethylfurfural | HCID 74191 | — |
Reaction Steps
5-Chloromethyl furfural was prepared by reaction of fructose with concentrated hydrochloric acid in toluene in a well-stirred two-phase system. The reaction was conducted at 85° C. for 10 minutes. The product was recovered by decanting the organic layer and removing toluene under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04433155 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-0baa075229dd40aa9b8125ce8aca8419 |
| Source note | uspto-grants-1984_02 |