HRID1388772

反应详情

EQUATION

反应方程式

HRID 1388772 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of ethyl P-methyl-2-nitrophenylphosphinate (10 mmol) in ethanol (40 ml) containing 10% palladium on carbon (200 mg) is hydrogenated at atmospheric pressure. After cessation of hydrogen uptake, the mixture is filtered and evaporated to dryness to give ethyl P-methyl-2-aminophenylphosphinate.

WORKUP

后处理

  1. filtrationAfter cessation of hydrogen uptake, the mixture is filtered
  2. customevaporated to dryness