2-Methoxybenzylamine → HCID 16769310, compound

HRID 1389153Notes

Reaction equation

HRID 1389153 reaction equation
C(OC([N:11]1[CH2:16][CH2:15][CH:14]([C:17](Cl)=[O:18])[CH2:13][CH2:12]1)=O)C1C=CC=CC=1.[CH3:20][O:21][C:22]1[CH:29]=[CH:28][CH:27]=[CH:26][C:23]=1[CH2:24][NH2:25]>>[CH3:20][O:21][C:22]1[CH:29]=[CH:28][CH:27]=[CH:26][C:23]=1[CH2:24][NH:25][C:17]([CH:14]1[CH2:13][CH2:12][NH:11][CH2:16][CH2:15]1)=[O:18]

Participants

3

Reactant 2

HCID 812922-MethoxybenzylamineHCID 2776270Benzyl 4-(chlorocarbonyl)piperidine-1-carboxylate

Product 1

HCID 16769310HCID 16769310, compound

Procedure

The above compound was prepared similarly to Preparation C starting from 1-benzyloxycarbonylpiperidine-4-carboxylic acid chloride and 2-methoxybenzylamine and had an m.p. of 139°-140°.

Workup

  1. customThe above compound was prepared similarly to Preparation C

Sources & evidence

ORD record
ord-b75dc7a84d314af6aa5c1576d810b015
Source dataset
uspto-grants-1981_01
Patent number
US04243666

Reaction notes

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