HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 20298522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Octylamine | HCID 8143 | — |
| Reactant | o-Cresol, 4-methylthio- | HCID 138054 | — |
| Product | HCID 20298522 | HCID 20298522 | 19% |
Reaction Steps
The epichlorohydrin derivative of 2-methyl-4-(methylthio)phenol (3.14 g., 0.015 mole) is reacted with n-octylamine (1.93 g. 0.015 mole) according to the procedure of Example 1. Concentrating the reaction mixture and crystallization of residual material from ethylacetate-hexane affords a 19% yield of analytically pure 1-[2-methyl-4-(methylthio)phenoxy]-3-(octylamino)-2-propanol, m.p. 59°-60° (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04243681 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-9af9e2f972ae4f0b81e4312a19525958 |
| Source note | uspto-grants-1981_01 |