Benzhydrylamine → HCID 20292147, compound

HRID 1389210Notes

Reaction equation

HRID 1389210 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7].[CH:11]([NH2:24])([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>C1CCCCC1>[CH:11]([NH:24][CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 2

HCID 7036BenzhydrylamineHCID 84580Ethyl 5-bromovalerate

Product 1

HCID 20292147HCID 20292147, compound

Reagents, catalysts & solvents 1

HCID 8078CyclohexaneSolvent

Procedure

25.1 g of ethyl 5-bromovalerate, 66 g of benzhydrylamine and 30 ml of cyclohexane are stirred at room temperature for 15 days. Processing analogously to Example 19 yields 23.4 (62.6%) of ethyl 5-benzhydrylaminovalerate [B.P. 158° to 163° (0.01 mm Hg)].

Sources & evidence

ORD record
ord-9642baf367b844d7a12c02c163bcb8e9
Source dataset
uspto-grants-1981_01
Patent number
US04243678

Reaction notes

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