4-Fluoroaniline → HCID 51776821, compound

Participants

Reaction Steps

The acid, N-(4-fluorophenyl)valine is prepared as above from 4-fluoroaniline and α-bromoisovaleric acid and then reacted with m-phenoxybenzyl bromide, as above, to yield the m-phenoxybenzyl ester of N-(4-fluorophenyl)valine. nmr (CDCl3) δ centered at 0.90 [m, 6, (CH3)2CH], 2.0 [m, 1, (CH3)2CH], 3.80 ##STR23## and 5.15 ppm (s, 2, ArCH2O). IR (film) 3400 m-1 (NH).

Provenance & Evidence