HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(p-chlorophenyl)valine → N-methyl,N-(4-chlorophenyl)valine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(p-chlorophenyl)valine | HCID 13796078 | — |
| Reactant | N-(4-methylphenyl)valine | HCID 53646739 | — |
| Product | N-methyl,N-(4-chlorophenyl)valine | HCID 70536039 | — |
Reaction Steps
Each of the m-phenoxybenzyl ester of N-(4-chlorophenyl)valine and N-(4-methylphenyl)valine is methylated using the procedure of Example 2 to yield the m-phenoxybenzyl ester of N-methyl,N-(4-chlorophenyl)valine, MS m/e 423 (M+), and the m-phenoxybenzyl ester of N-methyl,N-(4-methylphenyl)valine, MS m/e 403.2 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04243819 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-5c88aed80f054d2cadb2a2219fd42d7e |
| Source note | uspto-grants-1981_01 |