12-Hydroxystearic acid → HCID 12045785, compound

HRID 1389533Notes

Reaction equation

[OH:1][CH:2]([CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][C:13]([OH:15])=[O:14].[CH2:22](O)[CH:23]=[CH2:24]>>[CH2:24]([O:14][C:13](=[O:15])[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH:2]([OH:1])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])[CH:23]=[CH2:22]

Participants

Reactant 2

HCID 778912-Hydroxystearic acid

HCID 7858Allyl Alcohol

Product 1

HCID 12045785HCID 12045785, compoundYield 78%

Procedure

In analogy to A(2), 200 gm of 12-hydroxystearic acid were esterified with 300 ml of allyl alcohol. The 12-hydroxystearic acid allyl ester was obtained in a yield of 78%, and was distilled over in the high-vacuum at about 160° C. to 180° C.

Sources & evidence

ORD record: ord-60ec62423bd14393ae8d591103b4b600
Source dataset: uspto-grants-1981_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04245076

Reaction notes

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