HCID 20297209, compound → HCID 178482030, compound

HRID 1389592Notes

Reaction equation

HRID 1389592 reaction equation
[CH3:1][N:2]1[C:6]([S:7]([CH2:9][CH2:10][C:11]([OH:13])=O)=[O:8])=[N:5][N:4]=[N:3]1.[NH2:14][CH:15]1[C:32](=[O:33])[N:17]2[C:18]([C:29]([OH:31])=[O:30])=[C:19]([CH2:22][S:23][C:24]3[NH:28][N:27]=[N:26][CH:25]=3)[CH2:20][S:21][C@H:16]12>>[CH3:1][N:2]1[C:6]([S:7]([CH2:9][CH2:10][C:11]([NH:14][CH:15]2[C:32](=[O:33])[N:17]3[C:18]([C:29]([OH:31])=[O:30])=[C:19]([CH2:22][S:23][C:24]4[NH:28][N:27]=[N:26][CH:25]=4)[CH2:20][S:21][C@H:16]23)=[O:13])=[O:8])=[N:5][N:4]=[N:3]1

Participants

3

Reactant 2

HCID 20297209HCID 20297209, compoundHCID 178508102HCID 178508102, compound

Product 1

HCID 178482030HCID 178482030, compound

Procedure

408 mg. of 3-(1-methyl-1H-tetrazol-5-ylsulfinyl)propionic acid and 7-amino-3-(1H-1,2,3-triazol-5-ylthiomethyl)-3-cephem-4-carboxylic acid were reacted in the same manner as described in Example 28 and 120 mg. of 7-[3-(1-methyl-1H-tetrazol-5-ylsulfinyl)propionamido]-3-(1H-1,2,3-triazol-5-ylthiomethyl)-3-cephem-4-carboxylic acid were obtained.

Sources & evidence

ORD record
ord-757b2a43a4fe4bb5ab6ab33226b0b6be
Source dataset
uspto-grants-1981_01
Patent number
US04245107

Reaction notes

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