HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-phenylthio-2-(3-phenoxyphenyl)propionate → Methyl 2-(3-phenoxyphenyl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-phenylthio-2-(3-phenoxyphenyl)propionate | HCID 20556693 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Methyl 2-(3-phenoxyphenyl)propanoate | HCID 529082 | — |
Reaction Steps
330 mg of methyl 2-phenylthio-2-(3-phenoxyphenyl)propionate obtained in Example 8 was dissolved in 2 ml of acetic acid and the solution was heated while refluxing for 1 hour in the presence of 300 mg of zinc powder. After allowing the reaction mixture to cool, it was diluted with ethyl acetate and the remaining zinc powder was removed by filtration. The filtrate was concentrated to obtain methyl 2-(3-phenoxyphenyl)propionate in a quantative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04245108 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-5b4fc6e5ef894abcaba4e4bebf9fa3e2 |
| Source note | uspto-grants-1981_01 |