Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Tributylstannane | HCID 5948 | — |
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | HCID 20565023 | HCID 20565023 | — |
| Product | HCID 86735634 | HCID 86735634 | — |
Reaction Steps
To a stirred mixture of 31.5 g of 1-propargyl-1-trimethylsilyloxycyclohexane and 150 mg of azobisisobutyronitrile is added 41 ml of tri-n-butyltin hydride. The stirred mixture is heated to about 80° C. The initial exothermic reaction is moderated, and the temperature is subsequently maintained at 130°-135° C. for one hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04245121 |
|---|
| Source dataset | uspto-grants-1981_01 |
|---|
| ORD ID | ord-34b900a8c9e04d5692e50379ff0bce24 |
|---|
| Source note | uspto-grants-1981_01 |
|---|
