Methanol → HCID 20295707, compound

HRID 1389834Notes

Reaction equation

HRID 1389834 reaction equation
[CH3:1][C:2]1[CH2:7][CH2:6][CH2:5][C:4]([CH3:9])([CH3:8])[C:3]=1/[CH:10]=[CH:11]/[C:12]([CH3:14])=O.C[OH:16]>[Pd]>[CH3:1][CH:2]1[CH:3]([CH2:10][CH2:11][CH2:12][CH3:14])[C:4]([CH3:9])([CH3:8])[CH2:5][CH2:6][C:7]1=[O:16]

Participants

4

Reactant 2

HCID 887MethanolHCID 638014I2-Ionone

Product 1

HCID 20295707HCID 20295707, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

The mixture of compounds obtained according to example 1 starting from β-ionone is dissolved in methanol and hydrogenated at atmospheric pressure and room temperture using 5% Palladium on charcoal as a catalyst.

Workup

  1. additionThe mixture of compounds
  2. customobtained

Sources & evidence

ORD record
ord-ba31399aacaa4e3da259e9d8bb8bb58b
Source dataset
uspto-grants-1981_01
Patent number
US04246292

Reaction notes

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