HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 53897597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 86737448 | HCID 86737448 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53897597 | HCID 53897597 | — |
Reaction Steps
Equimolar amounts of 17-cyclopropylmethyl-7,7-dimethyl-3-hydroxy-6-oxamorphinan (XIV, prepared in Example 5), acetyl chloride and pyridine are mixed together in dry methylene chloride and heated at reflux temperature for 3 hours to produce the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04246413 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-aff3105debf7492d8e2e43a7ddc6a16c |
| Source note | uspto-grants-1981_01 |