HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 88766983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | N,N,N',N',N''-Pentamethylguanidine | HCID 139457 | — |
| Reactant | HCID 178511210 | HCID 178511210 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 88766983 | HCID 88766983 | 88% |
Reaction Steps
To a mixture of 0.1 mol of bis(2-cyanoethyl)phosphine oxide and 0.1 mol of acetone was added 1.0 gram of either triethyl amine or pentamethyl guanidine. The mixture was heated for 2 hours at steam bath temperatures. The resulting solid was filtered and recrystallized from acetone to give an 88% yield of product, m.p. 124°-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04247447 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-842a394f7c5a4c3cb602647f6bf0e708 |
| Source note | uspto-grants-1981_01 |