Sodium dimethylaminoethoxide → Bis(dimethylaminoethyl) ether

HRID 1389976Notes

Reaction equation

[CH3:1][N:2]([CH2:4][CH2:5][O:6]S([O-])(=O)=O)[CH3:3].[Na+].[CH3:12][N:13]([CH:15]([CH3:17])[O-])[CH3:14].[Na+]>>[CH3:1][N:2]([CH2:4][CH2:5][O:6][CH2:17][CH2:15][N:13]([CH3:14])[CH3:12])[CH3:3]

Participants

Reactant 2

HCID 86586345Sodium dimethylaminoethoxide

HCID 86737458Sodium dimethylaminoethylsulfate

Product 1

HCID 18204Bis(dimethylaminoethyl) ether

Procedure

subsequently, heating the resulting sodium dimethylaminoethylsulfate in the presence of sodium dimethylaminoethoxide to produce bis(N,N-dimethylaminoethyl)ether.

Sources & evidence

ORD record: ord-ea5e5994f5154589bd9bce73117dc135
Source dataset: uspto-grants-1981_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04247482

Reaction notes

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