2,5-Hexanedione → HCID 20294669, compound

HRID 1390001Notes

Reaction equation

HRID 1390001 reaction equation
Cl.Cl.[CH2:3]([N:6]([CH2:15][CH:16]=[CH2:17])[C:7]1[N:12]=[N:11][C:10]([NH:13][NH2:14])=[CH:9][CH:8]=1)[CH:4]=[CH2:5].C([O-])(=O)C.[Na+].[CH3:23][C:24](=O)[CH2:25][CH2:26][C:27](=O)[CH3:28]>C(O)(=O)C>[CH2:15]([N:6]([CH2:3][CH:4]=[CH2:5])[C:7]1[N:12]=[N:11][C:10]([NH:13][N:14]2[C:27]([CH3:28])=[CH:26][CH:25]=[C:24]2[CH3:23])=[CH:9][CH:8]=1)[CH:16]=[CH2:17]

Participants

5

Reactant 3

HCID 80352,5-HexanedioneHCID 2067223(2H)-Pyridazinone, 6-(di-2-propenylamino)-, hydrazone, dihydrochlorideHCID 517045Sodium Acetate

Product 1

HCID 20294669HCID 20294669, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

To 7 g (25 m moles) of 6-diallylamino-3-hydrazino-pyridazine dihydrochloride (Ger. Appl. 2.002.107; C.A. 73, 66596, 1970), and 4.1 g (50 m moles) of sodium acetate dissolved in 40 ml of acetic acid, 3.42 g (30 m moles) of 2,5-hexanedione are added.

Sources & evidence

ORD record
ord-7105df69d6f44983a378675809057109
Source dataset
uspto-grants-1981_01
Patent number
US04247551

Reaction notes

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