HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Butylamino-4-phenoxy-5-sulphamyl-benzamide → (4-Benzyl-3-n-butoxy-5-sulfamylbenzyl)dimethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Butylamino-4-phenoxy-5-sulphamyl-benzamide | HCID 21506065 | — |
| Reactant | 4-Benzyl-3-butoxy-N,N-dimethyl-5-sulfamoylbenzamide | HCID 54041480 | — |
| Product | (4-Benzyl-3-n-butoxy-5-sulfamylbenzyl)dimethylamine | HCID 54147820 | — |
Reaction Steps
By replacing in Example 289 3-n-butylamino-4-phenoxy-5-sulfamylbenzamide with an equimolar amount of 4-benzyl-3-n-butoxy-5-sulfamyl-N,N-dimethylbenzamide and following the procedure described, (4-benzyl-3-n-butoxy-5-sulfamylbenzyl)dimethylamine is obtained with a melting point of 110°-111° C. The material (IR, analysis) is identical with the material prepared as in Example 180.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04247550 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-cc26767ca5434538b84a8e712ecfacbd |
| Source note | uspto-grants-1981_01 |