HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Butylamino-4-phenoxy-5-sulphamyl-benzamide → (4-Benzyl-3-n-butoxy-5-sulfamylbenzyl)-2-diethylaminoethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Butylamino-4-phenoxy-5-sulphamyl-benzamide | HCID 21506065 | — |
| Reactant | 4-benzyl-3-n-butoxy-5-sulfamyl-N-(2'-diethylaminoethyl)-benzamide | HCID 54466401 | — |
| Product | (4-Benzyl-3-n-butoxy-5-sulfamylbenzyl)-2-diethylaminoethylamine | HCID 54157011 | — |
Reaction Steps
By replacing in Example 289 3-n-butylamino-4-phenoxy-5-sulfamylbenzamide with an equimolar amount of 4-benzyl-3-n-butoxy-5-sulfamyl-N-(2'-diethylaminoethyl)-benzamide and following the procedure described, (4-benzyl-3-n-butoxy-5-sulfamylbenzyl)-2-diethylaminoethylamine is obtained as a dihydrate with a melting point of 89°-93° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04247550 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-23b00d2b43fa47c3b57058ea36128642 |
| Source note | uspto-grants-1981_01 |