HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 22748383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 2-(4-Nitrophenoxy)ethanol | HCID 85381 | — |
| Reactant | HCID 22748384 | HCID 22748384 | — |
| Product | HCID 22748383 | HCID 22748383 | — |
Reaction Steps
By heating a mixture of 5 g of Intermediate 2, 12 g of β-(4-nitrophenoxy)ethanol, and 0.3 g of methanesulfonic acid to 140-150° C for 3 hours under a reduced pressure, the desired product was obtained. The solvent used for the recrystallization of the product was acetonitrile. The melting point of the product was 166-168° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04138258 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-82665e3cd41a4c1fa2780197c61572cc |
| Source note | uspto-grants-1979_02 |