HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 22748779, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Benzhydrol | HCID 7037 | — |
| Reactant | HCID 178516071 | HCID 178516071 | — |
| Product | HCID 22748779 | HCID 22748779 | — |
Reaction Steps
Combine 92.1 g (0.5 mole) of benzhydrol with 142.7 g. (1.5 mole) of 2-hydroxypyridine and heat to 190° C. with stirring. Add 1.5 ml. of concentrated sulfuric acid and follow the procedure of Example III, step A to obtain thereby the product of this step yield 68 g., m.p. 142°-145° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04138488 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-7f4404d8ea1a4a788420a938538dfd50 |
| Source note | uspto-grants-1979_02 |