HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → HCID 22749031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | N-amino-pyridinium chloride | HCID 12210597 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 22749031 | HCID 22749031 | 97% |
Reaction Steps
1-Aminopyridinium chloride (104 parts) and p-chlorobenzoyl chloride (150 parts) were heated in xylene (750 parts) at 140° C. for 4 hours. The solid product was filtered off and recrystallised from n-butanol to give 1-(p-chlorobenzamido)pyridinium chloride (209 parts, 97% yield), melting point 241° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04138548 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-e4f87846a5b245b88cafab35882fc4b8 |
| Source note | uspto-grants-1979_02 |