Propargyl bromide → HCID 86733430, compound

HRID 1390391Notes

Reaction equation

[CH3:1][CH:2]([O:9][C:10]1([OH:21])[CH:18]=[CH:17][C:13]([C:14]([OH:16])=[O:15])=[CH:12][CH:11]1[O:19][CH3:20])[CH2:3][CH2:4][CH2:5][CH:6]([CH3:8])[CH3:7].[CH2:22](Br)[C:23]#[CH:24]>>[CH2:24]([O:15][C:14](=[O:16])[C:13]1[CH:17]=[CH:18][C:10]([O:9][CH:2]([CH3:1])[CH2:3][CH2:4][CH2:5][CH:6]([CH3:7])[CH3:8])([OH:21])[CH:11]([O:19][CH3:20])[CH:12]=1)[C:23]#[CH:22]

Participants

Reactant 2

HCID 7842Propargyl bromide

HCID 70611998HCID 70611998, compound

Product 1

HCID 86733430HCID 86733430, compound

Procedure

By utilizing the procedure of Example 8, by reacting p-[(1,5-dimethylhexyl)oxy]vanillic acid with propargyl bromide, there is obtained p-[(1,5-dimethylhexyl)oxy]vanillic acid propargyl ester; nD24 = 1.5151.

Sources & evidence

ORD record: ord-1659c609102c4e838330d69eba30cbce
Source dataset: uspto-grants-1979_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04138579

Reaction notes

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