HRID1390533

反应详情

EQUATION

反应方程式

HRID 1390533 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
90 °C

PROCEDURE

实验过程

1-Nitro-9-phenoxyacridine (1.58 g) is dissolved in about 5 g of phenol, and then 0.95 g of 2-isobutylaminoethylamine dihydrochloride is added and is heated at a temperature of 90° C. for 1.2 hour. It is isolated in a similar manner, as in Example VII. There is obtained 1-nitro-9-isobutylaminoethylaminoacridine dihydrochloride with a melting point of 230° C. (with decomposition).

WORKUP

后处理

  1. customIt is isolated in a similar manner, as in Example VII