Aluminium lithium hydride → HCID 21332696, compound

HRID 1390555Notes

Reaction equation

HRID 1390555 reaction equation
[Cl:1][C:2]1[CH:17]=[CH:16][C:5]2[N+:6]([O-])=[N:7][C:8]3[CH:9]=[CH:10][C:11]([Cl:14])=[CH:12][C:13]=3[C:4]=2[CH:3]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[Cl:14][C:11]1[CH:10]=[CH:9][C:8]2[N:7]=[N:6][C:5]3[CH:16]=[CH:17][C:2]([Cl:1])=[CH:3][C:4]=3[C:13]=2[CH:12]=1

Participants

3

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 21332706HCID 21332706, compound

Product 1

HCID 21332696HCID 21332696, compound

Procedure

Furthermore, 2,9-dichloro-benzo-[c]-cinnoline is prepared according to the process described by J. F. Corbett, P. F. Holt, A. N. Hughes, M. Vickery (J. Chem. Soc. 1962, 1823) by the reduction of 2,9-dichloro-benzo-[c]-cinnoline-N-oxide with lithium aluminium hydride.

Sources & evidence

ORD record
ord-9fa2af2aa7884b568a6b651251f23b8f
Source dataset
uspto-grants-1979_02
Patent number
US04139530

Reaction notes

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