Methylhydrazine → HCID 70584361, compound

Participants

Reaction Steps

The product from Example 2 (5.8 g) was dissolved in methylene chloride (40 ml) and filtered to remove a trace of insoluble solids (0.15 g). The filtrate was cooled with an ice bath and treated under a nitrogen atmosphere with methylhydrazine (0.85 g, 18.7 mmol). The reaction was stirred 2 days under nitrogen at room temperature and then filtered to remove a solid, which was washed with a small amount of methylene chloride. The filtrate ws evaporated in vacuo to give 4.65 g of the title product.

Provenance & Evidence