Acetone → HCID 12789003, compound

HRID 1390824Notes

Reaction equation

HRID 1390824 reaction equation
Cl.[NH2:2][C:3]1[C:7]([C:8](=[O:10])[NH2:9])=[C:6]([CH3:11])[NH:5][C:4]=1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.[CH3:18][C:19]([CH3:21])=O>C(O)C.CCCCCC>[C:8]([C:7]1[C:3]([N:2]=[C:19]([CH3:21])[CH3:18])=[C:4]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[NH:5][C:6]=1[CH3:11])(=[O:10])[NH2:9]

Participants

4

Reactant 2

HCID 180AcetoneHCID 12339505HCID 12339505, compound

Product 1

HCID 12789003HCID 12789003, compoundYield 82%

Reagents, catalysts & solvents 1

HCID 21879635Ethanol hexaneSolvent

Procedure

From the compound of Example 33 and acetone, yield 82%, m.p. 221°-23° C. (from ethanol/hexane).

Sources & evidence

ORD record
ord-0a0b10af135a4dc2ac859f6b200db9c2
Source dataset
uspto-grants-1979_02
Patent number
US04140696

Reaction notes

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