HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 20330042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | HCID 12789002 | HCID 12789002 | — |
| Product | HCID 20330042 | HCID 20330042 | — |
Reaction Steps
By procedure (a) of Example 49 and starting from the compound of Example 46 and ethyl iodide, the 4-acetyl-3-benzylideneamino-1-ethyl-5-methyl-2-phenylpyrrole is obtained, m.p. 139°-41° C. (from isopropanol/water). This compound is hydrolyzed as in procedure (b) of Example 49. Overall yield of the title compound: 54%, m.p. 107°-8° C. (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04140696 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-46e082b6cbe649c1a50eebb807358f4c |
| Source note | uspto-grants-1979_02 |