HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Formylmorpholine → 4-Morpholinopyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Formylmorpholine | HCID 20417 | — |
| Reactant | 1,4'-Bipyridinium, chloride, hydrochloride (1:1:1) | HCID 79461 | — |
| Product | 4-Morpholinopyridine | HCID 4145413 | 59% |
Reaction Steps
With complete analogy to Examples 5 and 6, the reaction of 4-pyridylpyridinium chloride hydrochloride with N-formylmorpholine produced, in a 59% yield, 4-morpholinopyridine, m.p. 93-95° C. (from ligroin).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04140853 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-1a3cf75f260b4072b2a6c232405228e9 |
| Source note | uspto-grants-1979_02 |