HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl [2-(3-Hydroxypropyl)phenyl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | [2-(3-Hydroxypropyl)phenyl]acetic acid | HCID 20386052 | — |
| Product | Ethyl [2-(3-Hydroxypropyl)phenyl]acetate | HCID 53980166 | — |
Reaction Steps
A solution of [2-(3-hydroxypropyl)phenyl]acetic acid (48.6 g., 0.25 mole) and sulfuric acid (3 ml.) in ethanol (400 ml.) is heated at reflux for 6 hours. Workup as described in Example 25, Step A(3) yields the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04140861 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-5e18268077cc4611888227bf3181ca6c |
| Source note | uspto-grants-1979_02 |