HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178420865, compound → HCID 178485025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178420865 | HCID 178420865 | — |
| Reactant | HCID 178485082 | HCID 178485082 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178485025 | HCID 178485025 | 30.9% |
Reaction Steps
A solution of 1.23 g of 4,5,6,7-tetrahydro-imidazo-[4,5-c]-pyridine and 1.29 g of N,S-dimethyl-N'-cyano-isothiourea ##STR3## in 15 ml of acetonitrile is refluxed for 21 h. After evaporation to dryness, chromatography on silica gel (ethyl acetate-ethanol as eluant) of the residue gives 630 mg of the pure title compound, m.p. 240°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141899 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-b1360df3143e4eccab24670f1fe4c311 |
| Source note | uspto-grants-1979_02 |