4-Methyl-2-[2-(2-nitrophenyl)diazenyl]phenol → UV-328

HRID 1391254Notes

Reaction equation

HRID 1391254 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[N:10]=[N:11][C:12]1[CH:17]=[C:16]([C:18]([CH2:21][CH3:22])([CH3:20])[CH3:19])[CH:15]=[C:14]([C:23]([CH2:26][CH3:27])([CH3:25])[CH3:24])[C:13]=1[OH:28])([O-])=O.[N+](C1C=CC=CC=1N=NC1C=C(C)C=CC=1O)([O-])=O>>[OH:28][C:13]1[C:14]([C:23]([CH2:26][CH3:27])([CH3:25])[CH3:24])=[CH:15][C:16]([C:18]([CH2:21][CH3:22])([CH3:20])[CH3:19])=[CH:17][C:12]=1[N:11]1[N:10]=[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]2=[N:1]1

Participants

3

Reactant 2

HCID 740294-Methyl-2-[2-(2-nitrophenyl)diazenyl]phenolHCID 1041112-Nitro-2'-hydroxy-3',5'-bis(tert-amyl)azobenzene

Product 1

HCID 33263UV-328

Procedure

When using the procedure of Example 1 an equivalent amount of 2-nitro-2'-hydroxy-3',5'-di-tert-amylazobenzene is substituted for 2-nitro-2'-hydroxy-5'-methylazobenzene, the above noted product is obtained.

Workup

  1. customthe above noted product is obtained

Sources & evidence

ORD record
ord-2c7333093a8b4c06b2d6183b4680e700
Source dataset
uspto-grants-1979_02
Patent number
US04141903

Reaction notes

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