HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 21317477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 21317467 | HCID 21317467 | — |
| Product | HCID 21317477 | HCID 21317477 | — |
Reaction Steps
Lithium aluminum hydride reduction of the amide was accomplished according to the procedure of Example 5, giving 26.1 g of the 4-(5-(4-hydroxyphenylthio)pentyl)morpholine as a white solid. Recrystallization from ethanol gave the product as white crystals, mp 168°-171° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141983 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-5cc393df32ed4070867ad4baab20daa3 |
| Source note | uspto-grants-1979_02 |