HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → (3-Ethyl-2-hydroxyphenyl)(phenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | 3-Ethyl-2-hydroxybenzoyl chloride | HCID 45081581 | — |
| Product | (3-Ethyl-2-hydroxyphenyl)(phenyl)methanone | HCID 12562658 | 58.1% |
Reaction Steps
This compound (44.67 g) was prepared from benzene (172 g, 2.2 mole) and 2-hydroxy-3-ethyl benzoic acid chloride (63.15 g, 0.34 mole), using the same conditions as in Example 4. The b.p. of the compound was 123°-126° C./0.14 mm, ηD22 1.6081, γ max. (film) 1630 cm-1. The same compound was obtained using the method of Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04141995 |
| Source dataset | uspto-grants-1979_02 |
| ORD ID | ord-3c7f3bb54ed14dc398560c8d86240b1e |
| Source note | uspto-grants-1979_02 |