HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrafluoro-m-phenylenediamine dihydrochloride → HCID 69198399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Reactant | 2-Methyl-N-(4-nitrophenyl)-1-piperidinepropanamine | HCID 43080452 | — |
| Catalyst | ZINC ammonium chloride water ethanol | HCID 131726756 | — |
| Product | HCID 69198399 | HCID 69198399 | — |
Reaction Steps
The N-[3-(2-methylpiperidin-1-yl)propyl]-4-nitro-1-aminobenzene (17) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07338536B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-703b5f372c6542b781e1b75be166f321 |
| Source note | uspto-grants-2008_03 |