HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzenesulfonyl chloride → 3-(4-Methylpiperazine-1-sulfonyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzenesulfonyl chloride | HCID 8476 | — |
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Product | 3-(4-Methylpiperazine-1-sulfonyl)aniline | HCID 3197648 | — |
Reaction Steps
The title compound was prepared following the procedure of intermediate Example 2 with to 3-Nitro-benzenesulfonyl chloride (4.4 g, 20 mmol) and N-methyl-piperazine (2.2 ml 20 mmol) as an off white solid (3.6 g, 70%). MS (ESI) m/z=256 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07338959B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-e68686b8ea194533972a4d98240a12a3 |
| Source note | uspto-grants-2008_03 |