Benzenesulfonamide, 3-amino- → HCID 10289914, compound

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The title compound was prepared following the procedure of example one with N2-(4-Chloro-benzyl)-N5-(2-chloro-pyrimidin-4-yl)-1,N5-dimethyl-1H-benzoimidazole-2,5-diamine (103 mg, 0.25 mmol) and 3-amino-benzenesulfonamide (43 mg, 0.25 mmol) as a white solid (68 mg, 470%). 1H NMR (300 MHz, d6-DMSO+NaHCO3) δ 9.89 (br s, 1H), 8.49 (s, 1H), 7.86 (d, J=6.3 Hz, 1H), 7.73 (m, 1H), 7.18-7.74 (m, 10H), 5.73 (d, J=6.3 Hz, 1H), 4.71 (d, J=5.7 Hz, 2H), 3.69 (s, 3H), 3.47 (s, 3H). MS (ESI) m/z=549 [M+H]+.

Provenance & Evidence