4-Amino-N-methylbenzeneethanesulfonamide → HCID 69266082, compound

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The title compound was prepared following the procedure of example one with N2-(4-Chloro-benzyl)-N5-(2-chloro-pyrimidin-4-yl)-1,N5-dimethyl-1H-benzoimidazole-2,5-diamine (103 mg, 0.25 mmol) and 2-(4-amino-phenyl)-ethanesulfonic acid methylamide (54 mg, 0.25 mmol) as a white solid (96 mg, 64%). 1H NMR (300 MHz, d6-DMSO+NaHCO3) δ 10.27 (br s, 1H), 9.34 (br s, 1H), 7.85 (d, J=7.2 Hz, 1H), 7.61 (d, J=8.4 Hz, 1H), 7.49-7.54 (m, 4H), 7.38-7.44 (m, 3H), 7.20-7.26 (m, 3H), 6.99 (q, J=5.1 Hz, 1H), 5.83 (br s, 1H), 4.72 (d, J=5.7 Hz, 2H), 3.71 (s, 3H), 3.48 (s, 3H), 3.22-3.28 (M, 2H), 2.87-2.93 (m, 2H), 2.58 (d, J=4.8 Hz, 3H). MS (ESI) m/z=562 [M+H]+.

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