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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1391744Generated: November 2, 2026

4-Chlorophenylboronic acid → HCID 58629925, compound

https://huagongshe.com/reaction/1391744

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Chlorophenylboronic acidHCID 74299—
ReactantHCID 58629854HCID 58629854—
ProductHCID 58629925HCID 58629925—

Reaction Steps

Prepared according to the procedure used for the preparation of Intermediate 23, starting from ethyl [(4-{[1-(3-bromophenyl)pentyl]oxy}-2-methylphenyl)oxy]acetate (200 mg, 0.46 mmol) and 4-chlorobenzene boronic acid (86 mg, 0.55 mmol) to give, after purification by Biotage™ chromatography (silica, 40 g cartridge) eluting with petroleum ether 40-60° C.:EtOAc (19:1), the title compound (137 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07338960B2
Source datasetuspto-grants-2008_03
ORD IDord-73828089414546498bc752547162949f
Source noteuspto-grants-2008_03