HCID 10371682, compound → HCID 10459336, compound

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The compound {2-[(3S)-1-{(1S,2S)-1-[(2,4-Dimethyl-benzylamino)-methyl]-2-hydroxy-pentyl}-2-oxo-pyrrolidin-3-ylcarbamoyl]-4-trifluoromethyl-phenyl}-carbamic acid tert-butyl ester (9 mg) was dissolved in 3 mL of 2:1 CH2Cl2/TFA. The resultant solution was stirred for 3 h and then concentrated in vacuo. The residue was dissolved in TFA and concentrated in vacuo; this procedure was repeated. Lyopholization (H2O/MeCN) afforded the title compound as a white powder (5 mg). MS found: (M+H)+=521.5.

Provenance & Evidence