HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Mercapto-2-propanol → HCID 87765776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Mercapto-2-propanol | HCID 102545 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 10997510 | HCID 10997510 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 87765776 | HCID 87765776 | — |
Reaction Steps
11.68 g (67.8 mmol) of 3,4-diethoxythiophene, 12.5 g (135.6 mmol) of 1-mercapto-2-propanol and 1.29 g (6.8 mmol) of p-toluenesulphonic acid monohydrate were heated to reflux under an N2 atmosphere in 200 ml of toluene for 10 h. The further workup was as described in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07341801B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-6df948addda842e2bebc76eabef6b5e1 |
| Source note | uspto-grants-2008_03 |