HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Oxan-4-yl)methanesulfonyl chloride → 4-(Acetylthiomethyl)tetrahydropyran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Oxan-4-yl)methanesulfonyl chloride | HCID 18348392 | — |
| Reactant | 4-[4-(4-Fluorophenyl)piperazine-1-sulfonylmethyl]tetrahydropyran-4-carboxylic acid | HCID 22719726 | — |
| Reactant | 4-[4-(4-Fluorophenyl)piperazine-1-sulfonylmethyl]tetrahydropyran-4-carboxylic acid benzyl ester | HCID 69198807 | — |
| Product | 4-(Acetylthiomethyl)tetrahydropyran | HCID 59704018 | — |
Reaction Steps
MS (ESI): 331 (MNa+); 4-(chlorosulfonylmethyl)tetrahydropyran-4-(carboxylic acid benzyl ester): MS (ESI): 354 (MNa+); 4-[4-(4-fluorophenyl)piperazine-1-sulfonylmethyl]tetrahydropyran-4-carboxylic acid benzyl ester: MS (ESI): 477 (MH+), 499 (MNa+); 4-[4-(4-fluorophenyl)piperazine-1-sulfonylmethyl]tetrahydropyran-4-carboxylic acid: MS (ESI): 387 (MH+), 409 (MNa+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07342020B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-4455bc473f8b403f89529abfba0176da |
| Source note | uspto-grants-2008_03 |