14008-79-8 → HCID 131726801, compound

HRID 1392353Notes

Reaction equation

[CH3:1][N:2]1[CH:6]2[CH2:7][CH:8]([O:10][CH:11]([C:18]3[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=3)[C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[CH2:9][CH:3]1[CH2:4][CH2:5]2.[ClH:25].[CH3:26][C:27]1[O:33][C:32]([C:34]([NH:36][CH2:37][C:38]2[CH:43]=[CH:42][C:41]([C:44]3[CH:49]=[CH:48][CH:47]=[CH:46][CH:45]=3)=[CH:40][CH:39]=2)=[O:35])=[C:31]([OH:50])[C:29](=[O:30])[CH:28]=1>>[CH3:1][N:2]1[CH:6]2[CH2:7][CH:8]([O:10][CH:11]([C:18]3[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=3)[C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[CH2:9][CH:3]1[CH2:4][CH2:5]2.[ClH:25].[CH3:26][C:27]1[O:33][C:32]([C:34]([NH:36][CH2:37][C:38]2[CH:43]=[CH:42][C:41]([C:44]3[CH:49]=[CH:48][CH:47]=[CH:46][CH:45]=3)=[CH:40][CH:39]=2)=[O:35])=[C:31]([OH:50])[C:29](=[O:30])[CH:28]=1

Participants

Reactant 2

HCID 20313514008-79-8

HCID 54687474HCID 54687474, compound

Product 1

HCID 131726801HCID 131726801, compound

Procedure

According to the procedure for preparing FC-1/AM-1, but substituting AM-2 for AM-1, 50 g (41.29 mmol) of FC-1 was combined with 3.64 g (41.29 mmol) of AM-2 to provide FC-1/AM-2, nominal molecular weight=1267.15 g/mol.

Workup

customAccording to the procedure for preparing FC-1/AM-1

Sources & evidence

ORD record: ord-280d99fe766f431d84344bde01feee93
Source dataset: uspto-grants-2008_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07342080B2

Reaction notes

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