14008-79-8 → HCID 131726802, compound

HRID 1392354Notes

Reaction equation

HRID 1392354 reaction equation
[CH3:1][N:2]1[CH:6]2[CH2:7][CH:8]([O:10][CH:11]([C:18]3[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=3)[C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[CH2:9][CH:3]1[CH2:4][CH2:5]2.[ClH:25].[CH:26]1[CH:31]=[CH:30][C:29]([CH2:32][C:33]([NH:35][C:36]2[CH:41]=[C:40]([NH2:42])[CH:39]=[CH:38][C:37]=2[OH:43])=[O:34])=[CH:28][CH:27]=1>>[CH3:1][N:2]1[CH:6]2[CH2:7][CH:8]([O:10][CH:11]([C:18]3[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=3)[C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)[CH2:9][CH:3]1[CH2:4][CH2:5]2.[ClH:25].[CH:26]1[CH:27]=[CH:28][C:29]([CH2:32][C:33]([NH:35][C:36]2[CH:41]=[C:40]([NH2:42])[CH:39]=[CH:38][C:37]=2[OH:43])=[O:34])=[CH:30][CH:31]=1

Participants

3

Reactant 2

HCID 20313514008-79-8HCID 10263768HCID 10263768, compound

Product 1

HCID 131726802HCID 131726802, compound

Procedure

According to the procedure for preparing FC-1/AM-1, but substituting AM-4 for AM-1, 50 g (41.29 mmol) of FC-1 was combined with 4.80 g (20.64 mmol) of AM-4 and concentrated to provide FC-1/AM-4, nominal molecular weight 2590.4, nominal equivalent weight=647.6 g/mol.

Workup

  1. customAccording to the procedure for preparing FC-1/AM-1
  2. concentrationconcentrated

Sources & evidence

ORD record
ord-75432b9047744183820cd595da4afcc4
Source dataset
uspto-grants-2008_03
Patent number
US07342080B2

Reaction notes

Loading…