14008-79-8 → HCID 131726804, compound

HRID 1392356Notes

Reaction equation

[CH3:1][N:2]1[C:7](=[O:8])[C:6]([C:9]2[CH:14]=[CH:13][C:12]([O:15][C:16]3[CH:25]=[CH:24][N:23]=[C:22]4[C:17]=3[CH:18]=[C:19]([O:36][CH3:37])[C:20]([O:26][CH2:27][CH2:28][CH2:29][N:30]3[CH2:35][CH2:34][O:33][CH2:32][CH2:31]3)=[CH:21]4)=[C:11]([F:38])[CH:10]=2)=[CH:5][N:4]=[C:3]1[CH2:39][C:40]1[CH:45]=[CH:44][CH:43]=[CH:42][CH:41]=1.[CH3:46][N:47]1[CH:51]2[CH2:52][CH:53]([O:55][CH:56]([C:63]3[CH:68]=[CH:67][C:66]([Cl:69])=[CH:65][CH:64]=3)[C:57]3[CH:62]=[CH:61][CH:60]=[CH:59][CH:58]=3)[CH2:54][CH:48]1[CH2:49][CH2:50]2.[ClH:70]>>[CH3:46][N:47]1[CH:51]2[CH2:52][CH:53]([O:55][CH:56]([C:63]3[CH:68]=[CH:67][C:66]([Cl:69])=[CH:65][CH:64]=3)[C:57]3[CH:62]=[CH:61][CH:60]=[CH:59][CH:58]=3)[CH2:54][CH:48]1[CH2:49][CH2:50]2.[ClH:70].[CH3:1][N:2]1[C:7](=[O:8])[C:6]([C:9]2[CH:14]=[CH:13][C:12]([O:15][C:16]3[CH:25]=[CH:24][N:23]=[C:22]4[C:17]=3[CH:18]=[C:19]([O:36][CH3:37])[C:20]([O:26][CH2:27][CH2:28][CH2:29][N:30]3[CH2:35][CH2:34][O:33][CH2:32][CH2:31]3)=[CH:21]4)=[C:11]([F:38])[CH:10]=2)=[CH:5][N:4]=[C:3]1[CH2:39][C:40]1[CH:45]=[CH:44][CH:43]=[CH:42][CH:41]=1

Participants

Reactant 2

HCID 20313514008-79-8

HCID 11650194HCID 11650194, compound

Product 1

HCID 131726804HCID 131726804, compound

Procedure

To a 50-mL round-bottom flask, equipped with a magnetic stirbar, was charged 6.12 g (82.6 mmol) of AM-7 and 20 g (16.5 mmol) of FC-1 at room temperature. Next the mixture was stirred for about 30 min at room temperature. Finally volatiles were removed at temperatures up to 150° C. at 4.0 mm pressure to provide FC-1/AM-7, nominal molecular weight=1253.1 g/mol.

Workup

customTo a 50-mL round-bottom flask, equipped with a magnetic stirbar
customFinally volatiles were removed at temperatures up to 150° C. at 4.0 mm pressure

Sources & evidence

ORD record: ord-9decbd7155484c959866f1f53a926580
Source dataset: uspto-grants-2008_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07342080B2

Reaction notes

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