HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → 1-(1,1-Dimethyl-2-pyrrolidin-1-yl-ethyl)4-nitro-1H-imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 2-Methyl-2-(4-nitro-imidazol-1-yl)-propionaldehyde | HCID 86600809 | — |
| Product | 1-(1,1-Dimethyl-2-pyrrolidin-1-yl-ethyl)4-nitro-1H-imidazole | HCID 67165135 | — |
Reaction Steps
2-Methyl-2-(4-nitro-imidazol-1-yl)-propionaldehyde was reacted with pyrrolidine to provide the title compound: H1 NMR (400 MHz, CDCl3) 1.56 (s, 6H), 1.61 (m, 4H), 2.35 (m, 4H), 2.70 (m, 4H), 7.60 (s,1H), 7.92 (s, 1H); MS m/z 239.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07342118B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-8694a7f5ef8b4668a126a37d3e4b3c16 |
| Source note | uspto-grants-2008_03 |