HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethylmorpholine, cis- → 2,6-Dimethyl-4-[2-methyl-2-(4-nitro-imidazol-1-yl)-propyl]-morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethylmorpholine, cis- | HCID 641500 | — |
| Reactant | 2-Methyl-2-(4-nitro-imidazol-1-yl)-propionaldehyde | HCID 86600809 | — |
| Product | 2,6-Dimethyl-4-[2-methyl-2-(4-nitro-imidazol-1-yl)-propyl]-morpholine | HCID 67164043 | — |
Reaction Steps
2-Methyl-2-(4-nitro-imidazol-1-yl)-propionaldehyde was reacted with cis-2,6-dimethyl morpholine to provide the title compound: C13 NMR (100 MHz, CDCl3) 19.0, 25.7, 60.8, 61.5, 68.5, 72.0, 118.0, 134.5; MS m/z 283.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07342118B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-a2b0578a18b14d95b3d8d2aaa70a9d08 |
| Source note | uspto-grants-2008_03 |