HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 66993803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 59678289 | HCID 59678289 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66993803 | HCID 66993803 | — |
Reaction Steps
A mixture of [6-(2,6-diethyl-phenyl)-4-ethoxy-2-methyl-pyridin-3-yl]-methanol (1.8 g) and SOCl2 (2 mL) in CH2Cl2 (10 mL) is stirred at room temperature for one hour. The volatile materials are removed in vacuo to give 3-chloromethyl-6-(2,6-diethyl-phenyl)-4-ethoxy-2-methyl-pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07342115B2 |
| Source dataset | uspto-grants-2008_03 |
| ORD ID | ord-a38936e84c33448f8fa49e8427523492 |
| Source note | uspto-grants-2008_03 |